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العنوان
Design, Structural Investigation, DNA Interaction, Antimicrobial and Anticancer Activities of Some New Ag(I), VO(II) and Pd(II|) Complexes Encompassing Chemosensor Imine Ligand /
المؤلف
Abdel-Mawgood, Azza Ahmed Hassan.
هيئة الاعداد
مشرف / ليلى حمدان عبدالرحمن
مشرف / احمد محمد ابو ضيف
ahmed.mohamed7@science.sohag.edu.eg
مشرف / سحر ابراهيم حامد مصطفى
saharmostafa@mans.edu.eg
مشرف / مجدي شبل صالح السيد
باحث / عزه احمد حسن
الموضوع
Dna interaction.
تاريخ النشر
2019.
عدد الصفحات
p. 333 :
اللغة
الإنجليزية
الدرجة
الدكتوراه
التخصص
Inorganic Chemistry
تاريخ الإجازة
30/11/2019
مكان الإجازة
جامعة سوهاج - كلية العلوم - كيمياء
الفهرس
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Abstract

Air and moisture stable coordination compounds of some transition metal ions such as Ag (I), VO (II) and Pd (II) with newly designed bi- and tri-dentate imine ligands (NBA, HNAP, HNA and DAPH) were synthesized. Bi-dentate imine ligands
(NBA, HNAP) were synthesized by reacting 3-nitro benzaldehyde
(NB) or 2-hydroxynapthaldehyde (HN) with 2-amino benzoic acid
(A) or 3-amino pyridine (AP), respectively. Whereas tri-dentate
imine ligands (HNA and DAPH) were prepared by reacting 2-
hydroxy-1-napthaldehyde (HN) or 2,6 diacetyl pyridine (DA) with
2-amino benzoic acid (A) or phenyl hydrazine hydrochloride
(PH), respectively. All the prepared imine ligands were analyzed
by their melting points, 1HNMR,
13CNMR spectra, elemental
analyses, UV-Vis and IR spectra. The data obtained from spectral
investigation especially 1H and 13CNMR confirmed the formation
of azomethine nitrogen in the ligands structure. Molecular
structures of the prepared imine complexes were identified by
several techniques including mass spectra, elemental analyses, IR.